DETERMINACIÓN DE FLUOROQUINOLONAS EN TEJIDO ANIMAL MEDIANTE CROMATOGRAFÍA LÍQUIDA ACOPLADA A ESPECTROMETRÍA DE MASAS
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Publicado:
ago 30, 2015
Palabras clave:
Espectrometría de Masas; Fluoroquinolonas; Prueba de Aptitud; Z-score; Mass Spectrometry; Fluoroquinolone; Proficiency test; Z-score
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Resumen
Un método multiresiduos, para la determinación simultánea de Fluoroquinolonas ácidas y básicas en tejido animal ha sido desarrollado mediante UPLC/MS/MS; con recuperaciones en el orden del 93 a 108%. Se establecieron LOD =5,0 ngg-1 y LOQ =10,0 ngg-1 para cada quinolona. La robustez del método permite su aplicación a varios tipos de matrices como camarón, pescado, pavo, etc.
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Fernando Gualpa Jaramillo, Michael Rendón Morán. DETERMINACIÓN DE FLUOROQUINOLONAS EN TEJIDO ANIMAL MEDIANTE CROMATOGRAFÍA LÍQUIDA ACOPLADA A ESPECTROMETRÍA DE MASAS. EEC [Internet]. 30 de agosto de 2015 [citado 22 de diciembre de 2024];2(2). Disponible en: https://revistaecuadorescalidad.agrocalidad.gob.ec/revistaecuadorescalidad/index.php/revista/article/view/14
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Artículos Científicos
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S. Nseir, C. Di Pompeo, S. Soubrier, P. Delour, H. Lenci, M. Roussel-Delvallez, A. Durocher (2005). “First-generation fluoroquinolone use and subsequent emergence of multiple drug-resistant bacteria in the intensive care unit”. Critical care medicine, 33(2), 283-289.
J. M. Blondeau (2004). “Fluoroquinolones: mechanism of action, classification, and development of resistance”. Survey of ophthalmology, 49(2), S73-S78.
P. Gigosos, P. Revesado, O. Cadahıa, C. Fente, B. Vazquez, C. Franco, & A. Cepeda. (2000). Determination of quinolones in animal tissues and eggs by high-performance liquid chromatography with photodiode-array detection. Journal of chromatography A, 871(1), 31-36.
I. Jiménez-Díaz, M. Hermo, O. Ballesteros, A. Zafra-Gómez, D. Barrón, J. Barbosa, & A. Navalón. (2013). Comparison of three analytical methods for the determination of quinolones in pig muscle samples. Chromatographia, 76(11-12), 707-713.
Martins, Magda Targa, et al. (2015). "Determination of quinolones and fluoroquinolones, tetracyclines and sulfonamides in bovine, swine and poultry liver using LC-MS/MS." Food Additives & Contaminants: Part A, 32.3, 333-341.
M. Wagil, et al. (2014). "Development of sensitive and reliable LC-MS/MS methods for the determination of three fluoroquinolones in water and fish tissue samples and preliminary environmental risk assessment of their presence in two rivers in northern Poland." Science of the Total Environment, 493, 1006-1013.
Rezk, R. Mamdouh, et al. (2015). "Multi-residues determination of antimicrobials in fish tissues by HPLC–ESI-MS/MS method." Journal of Chromatography B, 978, 103-110.
Tsai, Chung-Wei, Chan-Shing Lin, and Wei-Hsien Wang. (2012). "Multi-Residue Determination of Sulfonamide and QuinoloneResidues in Fish Tissues by High Performance LiquidChromatography-Tandem Mass Spectrometry (LC-MS/MS)." 藥物食品分析 20.3, 674-680.
Regulation, C. (2010). “No. 37/2010 of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin”, Off. J. Eur. Union L, 15, 1-72.
K. M. Jenkins, M. S. Young (2004). “LC-MS determination of fluoroquinolone antibiotics in beef tissue using the Atlantis (R) dC (18) column”, LC GC EUROPE, 17(11 A), 53-54.
M. J. Schneider, D. J. Donoghue (2003). “Multiresidue determination of fluoroquinolone antibiotics in eggs using liquid chromatography–fluorescence–mass spectrometry n”, Analytica chimica acta, 483(1), 39-49.
J. Shen, L. Guo, F. Xu, Q. Rao, X. Xia, X. Li, & S. Ding. (2010). “Simultaneous Determination of Fluoroquinolones, Tetracyclines and Sulfonamides in Chicken Muscle by UPLC–MS–MS”. Chromatographia, 71(5-6), 383-388.
W. Guo, Y. Liu, & N. Liu. (2009). “Simultaneous analysis of 7 fluoroquinolone residues in chicken muscle by ultra performance liquid chromatography-electrospray ionization tandem mass spectrometry”. Chinese journal of chromatography/Zhongguo hua xue hui, 27(4), 406-411.
N. Van Hoof, K. De Wasch, L. Okerman, W. Reybroeck, S. Poelmans, H. Noppe, & H. De Brabander. (2005). “Validation of a liquid chromatography–tandem mass spectrometric method for the quantification of eight quinolones in bovine muscle, milk and aquacultured products”. Analytica Chimica Acta, 529(1), 265-272.
G. Dufresne, A. Fouquet, D. Forsyth, & S. A.Tittlemier, (2007). “Multiresidue determination of quinolone and fluoroquinolone antibiotics in fish and shrimp by liquid chromatography/tandem mass spectrometry”. Journal of AOAC International, 90(2), 604-612.
S. Nseir, C. Di Pompeo, S. Soubrier, P. Delour, H. Lenci, M. Roussel-Delvallez, A. Durocher (2005). “First-generation fluoroquinolone use and subsequent emergence of multiple drug-resistant bacteria in the intensive care unit”. Critical care medicine, 33(2), 283-289.
J. M. Blondeau (2004). “Fluoroquinolones: mechanism of action, classification, and development of resistance”. Survey of ophthalmology, 49(2), S73-S78.
P. Gigosos, P. Revesado, O. Cadahıa, C. Fente, B. Vazquez, C. Franco, & A. Cepeda. (2000). Determination of quinolones in animal tissues and eggs by high-performance liquid chromatography with photodiode-array detection. Journal of chromatography A, 871(1), 31-36.
I. Jiménez-Díaz, M. Hermo, O. Ballesteros, A. Zafra-Gómez, D. Barrón, J. Barbosa, & A. Navalón. (2013). Comparison of three analytical methods for the determination of quinolones in pig muscle samples. Chromatographia, 76(11-12), 707-713.
Martins, Magda Targa, et al. (2015). "Determination of quinolones and fluoroquinolones, tetracyclines and sulfonamides in bovine, swine and poultry liver using LC-MS/MS." Food Additives & Contaminants: Part A, 32.3, 333-341.
M. Wagil, et al. (2014). "Development of sensitive and reliable LC-MS/MS methods for the determination of three fluoroquinolones in water and fish tissue samples and preliminary environmental risk assessment of their presence in two rivers in northern Poland." Science of the Total Environment, 493, 1006-1013.
Rezk, R. Mamdouh, et al. (2015). "Multi-residues determination of antimicrobials in fish tissues by HPLC–ESI-MS/MS method." Journal of Chromatography B, 978, 103-110.
Tsai, Chung-Wei, Chan-Shing Lin, and Wei-Hsien Wang. (2012). "Multi-Residue Determination of Sulfonamide and QuinoloneResidues in Fish Tissues by High Performance LiquidChromatography-Tandem Mass Spectrometry (LC-MS/MS)." 藥物食品分析 20.3, 674-680.
Regulation, C. (2010). “No. 37/2010 of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin”, Off. J. Eur. Union L, 15, 1-72.
K. M. Jenkins, M. S. Young (2004). “LC-MS determination of fluoroquinolone antibiotics in beef tissue using the Atlantis (R) dC (18) column”, LC GC EUROPE, 17(11 A), 53-54.
M. J. Schneider, D. J. Donoghue (2003). “Multiresidue determination of fluoroquinolone antibiotics in eggs using liquid chromatography–fluorescence–mass spectrometry n”, Analytica chimica acta, 483(1), 39-49.
J. Shen, L. Guo, F. Xu, Q. Rao, X. Xia, X. Li, & S. Ding. (2010). “Simultaneous Determination of Fluoroquinolones, Tetracyclines and Sulfonamides in Chicken Muscle by UPLC–MS–MS”. Chromatographia, 71(5-6), 383-388.
W. Guo, Y. Liu, & N. Liu. (2009). “Simultaneous analysis of 7 fluoroquinolone residues in chicken muscle by ultra performance liquid chromatography-electrospray ionization tandem mass spectrometry”. Chinese journal of chromatography/Zhongguo hua xue hui, 27(4), 406-411.
N. Van Hoof, K. De Wasch, L. Okerman, W. Reybroeck, S. Poelmans, H. Noppe, & H. De Brabander. (2005). “Validation of a liquid chromatography–tandem mass spectrometric method for the quantification of eight quinolones in bovine muscle, milk and aquacultured products”. Analytica Chimica Acta, 529(1), 265-272.
G. Dufresne, A. Fouquet, D. Forsyth, & S. A.Tittlemier, (2007). “Multiresidue determination of quinolone and fluoroquinolone antibiotics in fish and shrimp by liquid chromatography/tandem mass spectrometry”. Journal of AOAC International, 90(2), 604-612.